fn1_lg_14_spectroscopy.doc
fn1_2f_spectroscopy.ppt

If you don't have X-ray spectroscopy your SEM just isn't complete. In this module I cover X-ray analysis and mass spectometery. For the laboratory activity I just have them run and X-ray analysis on a variety of metal samples. For the lecture portion I describe the operation of the energy dispersive X-ray detector (EDS sometimes called EDX) and the wavelength dispersive X-ray Detectro (WDS). I want them to no about the pile up rejector and how it gives rise to dead time. The trade off between accumulation time, resolution and dead time. I also want them to know why WDS might be preferred over EDS and how thermionic vs. field emission influences the x-ray counts. I can show them how to do an elemental map and identify the different types of atoms/elements in the sample.

For the next part I do a survey of spectroscopy and spectometry. I am probably spending too much time on this but there is such a variety of surface analysis equipment out there that it is hard to included it all. Some that I consider important are Mass Spec, ICP-MS, SIMS, FIB, Atom Probe Microscopy, FTIR, Raman. I also briefly cover XPS. I am saving allowed electron transitions in X-ray generation for a later section. I will also cover XRD later. I want to finish up with the tools for now and move on to Nanomaterials which is a nice change and keeps the students interested.

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Publications by A. Paszternák:

The potential use of cellophane test strips for the quick determination of food colours

pH and CO2 Sensing by Curcumin-Coloured Cellophane Test Strip

Polymeric Honeycombs Decorated by Nickel Nanoparticles

Directed Deposition of Nickel Nanoparticles Using Self-Assembled Organic Template,

Organometallic deposition of ultrasmooth nanoscale Ni film,

Zigzag-shaped nickel nanowires via organometallic template-free route

Surface analytical characterization of passive iron surface modified by alkyl-phosphonic acid layers

Atomic Force Microscopy Studies of Alkyl-Phosphonate SAMs on Mica

Amorphous iron formation due to low energy heavy ion implantation in evaporated 57Fe thin films

Surface modification of passive iron by alkylphosphonic acid layers

Formation and structure of alkylphosphonic acid layers on passive iron

Structure of the nonionic surfactant triethoxy monooctylether C8E3 adsorbed at the free water surface, as seen from surface tension measurements and Monte Carlo simulations