"Spicy world of NanoScience"
DEAR FRIENDS,
I have prepared Copper Nanoparticles in DI Water and want to separate them from solution. Kindly tell me the simple way to separate and dry these particles.
Thanks.
Asim Umer
Tags: copper, nanoparticles, seprataion, solution
Permalink Reply by Dr.Claudio Gutiérrez on June 3, 2012 at 7:10am I have not experience on synthesis and manipulation of metallic colloids, but a simple separation process is the use of nonsolvent aliquots (normally alcohols, depending of your surfactant) on colloidal solution, accompanied of centrifugal treatments and using desiccator, May be, this paper can be useful.
http://www.nanoscalereslett.com/content/4/5/465
Permalink Reply by Naren on June 3, 2012 at 7:29am
Permalink Reply by Satyendra Kumar on June 4, 2012 at 11:44am You can use microemulsion method for the synthesis of nanoparticles
Permalink Reply by MADAN IYENGAR on June 6, 2012 at 5:05pm
Permalink Reply by Don Baer on June 6, 2012 at 5:13pm Depending on your needs, you might find the following paper of some value: J. T. Nurmi et al. "Recovery of Iron/Iron Oxide Nanoparticles from Solution: Comparison of Methods and their Effects" Journal of Nanoparticle Research 2011 13(5) 1937-1952.
Permalink Reply by Dr. Vandna Luthra on June 6, 2012 at 6:14pm You can use centrifuging at 5000-6000 rpm for 10-15 minutes. This
can be further dried at moderate temperature. Also it would be good to
use alcohols.
All the best.
Permalink Reply by HALA ELHADI MOHD on June 6, 2012 at 9:56pm I have not experience on the copper , but h hope good luck for you dear>>>> i have qesution for what you need copper NPS????????????
Permalink Reply by TamilSelvi on June 7, 2012 at 4:36am hello!
First u have to centrifuge your sample . you try the rpm range from 3000 to 10,000 rpm depending up on your particle size. larger the particle size lower rpm is enough. Then you can see the copper nanoparticle at the bottom remove the filtrate. Further the trace of the solvent is removed by vacuum. if u heat to remove water some times nanoparticle change it's morphology.
Permalink Reply by D. Geethalakshmi on June 7, 2012 at 5:51am centrifuge it for many times to remove excess DI water and form as a slury. then pour it on petridish and dry it in proper environmental condition which u need.


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