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Now i am working in Ag@SiO2 core shell nanoparticle Preparation. I am not getting core shell structure did same mistake repeatly. I couldnt find my fault.

This my procedure, First i prepared citrate & PVP stabilished Silver nanoparticle. 1 ml of ag collide in 10 ml water after that i add TEOS & ammonia/NaoH.

Please help me..

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Sir, I think you have to change the stabilizer, instead of citrate and PVP just try out with mercaptosuccinic acid. The stabilizers you have used might be bulky enough to prevent the bonding of SiO2 with Ag

Hi Friend,

I will try that one. Thank you so much for ur suggestion.

 

Thanking You,

 

With Regards,

 

Saravanakumar

 

How is the structure of your product?

 

Dieter Vollath

Dear Professor,

Thank You very much for replying.  after addition of TEOS Ag nanoparticles aggregates.If Possible send the Email iD Prof. I will send my TEM Images.

 

Thanking You,

 

With Regards,

 

Saravanakumar

dieter.vollath@nanoconsulting.de

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